FE-SEM Preliminary

1. Swipe into the computer logbook to activate the microscope.


Liquid nitrogen metal dewar.

2. Fill cold trap dewar on SEM with 5–6 funnels of liquid nitrogen.


Metal funnel near the FE-SEM system.

Funnel.


EDS with out position marked on a ruler and on a label.

3. Check that the EDS detector is in the "out" position at 6.


4. The computer will already be logged on. Do not change the log-in. You cannot log in to your home directory.


5. Click on the S-4700 icon to start the software. You do not need a password. Just click "OK".


Stage XY Position Set

6. The software will display a window with stage coordinates. The proper coordinates are: X = 12.5 mm, Y = 12.5 mm, and Z = 12 mm. Check that the software stage coordinates agree with the actual stage position. If not, adjust the stage by hand and make any required changes to the display window. Click "OK".


Operating Procedure: Specimen Exchange